|
Materials Science and Engineering Department,
University of Florida, P.O. Box 116400, Gainesville, FL 32611, USA
* Corresponding author: Tel. 1-352-846-3791, Fax:1-352-846-3355,
e-mail: febra@mse.ufl.edu
Nanocrystalline Ni-Fe alloys with composition in the 5wt% to 50 wt% Fe range were fabricated via the electrodeposition method. Very fine grain size (»approx. 11nm) with nearly random crystallographic orientation was obtained in alloys with equal or more than 15wt% Fe. For a nominally constant grain size, the hardness of the deposits decreased and the level of internal stresses increased with raising the iron content above 15wt%. At low iron concentrations, the deposit showed large grain size with a strong <100> texture. These observations are discussed in terms of the development of the structure during the deposition process. |
full paper (pdf, 150 Kb)